HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 69516270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | HCID 58932670 | HCID 58932670 | — |
| Product | HCID 69516270 | HCID 69516270 | — |
Reaction Steps
The title compound was obtained as an off-white solid (37.3 mg, 17.6%), mp>275° C. from compound 1C and 4-hydroxybenzaldehyde in the same manner as that used in the preparation of Example 1 by acidifying the aqueous washings and recrystallization of the crude product from MeOH. LC/MS m/z 356 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07256208B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-6df4a666734349d39a2d6b2a41ee5c98 |
| Source note | uspto-grants-2007_08 |