huagongshe.com
HRID853910

反应详情

EQUATION

反应方程式

HRID 853910 的结构方程式

REACTANTS

反应物

2
结构：N#CC1(CCl)CCCCC1
HCID2794920

1-(Chloromethyl)Cyclohexanecarbonitrile

C8H12ClN

结构：O=C1Nc2ccc(S(=O)(=O)N3CCC[C@H]3COc3ccccc3)cc2C12OCCCO2
HCID25269014

未命名化合物

PRODUCTS

生成物

1
结构：O=C1C2=NCC3(CCCCC3)CN2c2ccc(S(=O)(=O)N3CCC[C@H]3COc3ccccc3)cc21
HCID11496899

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as a yellow foam from 5′-{[(2S)-2-(phenoxymethyl)pyrrolidin-1-yl]sulfonyl}spiro[1,3-dioxane-2,3′-indol]-2′(1′H)-one and 1-chloromethyl-cyclohexanecarbonitrile (Syn. Comm. 20(12) 1757, 1990) using a procedure similar to that of steps 3-5 of Example 12. NMR (400 Mz, DMSO-d6): consistent. MS: (ES−) m/z 492 [M−H]