3-Methoxybenzaldehyde → HCID 85326139, compound

Participants

Reaction Steps

The title compound was prepared from a mixture of 2,5-bis(2,2,2-trifluoroethoxy)acetophenone (200 mg, 0.633 mmol) and m-anisaldehyde (77 ul, 0.633 mmol) similar to Example 6 and isolated as a light yellow solid (74 mg, 27%). 1H NMR (CDCl3): 7.67 (d, J=15.6 Hz, 1H), 7.44 (d, J=15.6 Hz, 1H), 7.34 (s, 1H), 7.30 (dd, J=2.4, 5.7 Hz, 1H), 7.18 (d, J=7.5 Hz, 1H), 7.11 (dd, J=3.2, 8.9 Hz, 2H), 6.97 (dd, J=0.9, 2.7 Hz, 1H), 6.93 (d, J=9.0 Hz, 1H), 4.44-4.33 (m, 4H), 3.83 (s, 3H).

Provenance & Evidence