3-Methylbenzaldehyde → HCID 90723180, compound

Participants

Reaction Steps

The title compound was prepared from a mixture of 2,5-bis(2,2,2-trifluoroethoxy)acetophenone (200 mg, 0.633 mmol) and m-tolualdehyde (75 ul, 0.633 mmol) similar to Example 6 and isolated as a pale yellow solid (76.2 mg, 29%). 1H NMR (CDCl3): 7.66 (d, J=15.9 Hz, 1H), 7.44 (d, J=15.6 Hz, 1H), 7.42-7.38 (m, 2H), 7.31-7.20 (m, 3H), 7.10 (dd, J=3.2, 8.9 Hz, 1H), 6.93 (d, J=9.0 Hz, 1H), 4.43-4.32 (m, 4H), 2.37 (s, 3H).

Provenance & Evidence