2-Pyridinecarboxaldehyde → HCID 85331303, compound

Participants

Reaction Steps

The title compound was prepared from a mixture of 2,5-bis(2,2,2-trifluoroethoxy)acetophenone (100 mg, 0.316 mmol) and 2-pyridine carboxaldehyde (30 ul, 0.316 mmol) similar to Example 15 and isolated as a yellow solid (13 mg, 10%) 1H NMR (CDCl3): 8.68-8.65 (m, 1H), 7.79 (d, J=15.6 Hz, 1H), 7.72 (dd, J=1.7, 7.7 Hz, 1H), 7.64 (d, J=15.6 Hz, 1H), 7.53 (d, J=7.8 Hz, 1H), 7.31-7.28 (m, 1H), 7.25 (s, 1H), 7.12 (dd, J=3.2, 8.9 Hz, 1H), 6.96 (d, J=9.3 Hz, 1H), 4.44-4.33 (m, 4H).

Provenance & Evidence