HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22998584, compound → HCID 22998664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22998584 | HCID 22998584 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22998664 | HCID 22998664 | 127.4% |
Reaction Steps
2-(4-Benzylpiperazin-1-yl)methyl-6-methoxytetralin dihydrochloride (0.849 g) was added to conc. hydrochloric acid (20 ml) and the reaction mixture was heated under reflux for 6 hr and cooled. The resulting precipitate was collected and washed with ethanol, methanol, and diethyl ether to obtain the titled compound (0.523 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07256204B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-867f7d332a254144b2c27a2b0ab1bad2 |
| Source note | uspto-grants-2007_08 |