HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131726552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69156110 | HCID 69156110 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131726552 | HCID 131726552 | — |
Reaction Steps
A solution of (3R,7R)-4-[(3R)-3-[(tert-butoxycarbonyl)amino]-4-(2,4,5-trifluorophenyl)butanoyl]-3,7-dimethyl-1,4-diazepan-2-one (175 mg, 0.38 mmol) in 4 mL of 4N hydrogen chloride in dioxane (4 mL, 4N) was stirred for 2 h and concentrated. The residue was dried under vacuum overnight to yield the title compound as a white solid. MS 358.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07259160B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-75e1798cc571455e86e336cc57dedd1d |
| Source note | uspto-grants-2007_08 |