HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 86598513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | 4-Methoxybenzenecarbothioamide | HCID 736827 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86598513 | HCID 86598513 | 119% |
Reaction Steps
13.38 g (80.0 mmol) 4-Methoxy-thiobenzamide, 15.23 g (120 mmol) 1,3-dichloroacetone and 400 ml acetone were stirred at room temperature for 3 days. The precipitate was isolated and dried, yielding 21.0 g (quant.) 4-methoxy-thiobenzimidic acid 3-chloro-2-oxo-propyl ester hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07259262B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-ea6ab41a820945ec9d6d3ca7cea9189e |
| Source note | uspto-grants-2007_08 |