1,3-Dichloroacetone → HCID 86598514, compound

Participants

Reaction Steps

2.30 g (9.95 mmol) 3-(4-Trifluoromethyl-phenyl)-acrylthioamide, 2.52 g (19.90 mmol) 1,3-dichloroacetone and 75 ml acetone were stirred at room temperature for 24 h. The precipitate was isolated and dried, yielding 2.50 g (70%) 3-(4-trifluoromethyl-phenyl)-thioacrylimidic acid 3-chloro-2-oxo-propyl ester hydrochloride.

Provenance & Evidence