Hydrochloric Acid → HCID 69492514, compound

Participants

Reaction Steps

1.4 g of (R)-2-(2-{4-[2-(4-Hexyloxy-phenyl)-vinyl]-benzyloxy}-1-phenyl-ethoxy)-tetrahydro-pyran (4) were dissolved in 30 ml of ethanol. Hydrochloric acid was added dropwise to obtain an acidic medium. Then the mixture was refluxed for 30 min. Upon cooling the product crystallized. The solid was filtered, washed with ethanol, and dried in a dessicator.

Provenance & Evidence