HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 855465Generated: October 29, 2026
4-Methoxyphenol → HCID 23516352, compound
https://huagongshe.com/reaction/855465
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | HCID 58935103 | HCID 58935103 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23516352 | HCID 23516352 | — |
Reaction Steps
98.5 g (0.2 mole) of ethoxymethyl 4-(4-(6-acryloyloxyhexyloxy)bezoyloxy)benzoate (16) were dissolved in 400 ml of ethanol and 5 g (0.02 mole) of pyridinium 4-toluensulfonate and 20 mg of 4-methoxyphenol were added. The mixture was heated at 60° C. for 15 h. After cooling down at room temperature the product crystallized. It was collected, washed with 300 ml of ethanol, and dried in a desiccator 55.3 g of a white powder (67%) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07261836B2 |
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| Source dataset | uspto-grants-2007_08 |
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| ORD ID | ord-c7e3d486a2f946e1af110cddf6235b3c |
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| Source note | uspto-grants-2007_08 |
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