Sodium Chloride → HCID 69516387, compound

Participants

Reaction Steps

200 mg (5.25 mmol) of LiAlH4, in small portions, are added to a solution containing 485 mg (1.31 mmol) of the compound of Step A above in 15 ml of THF. After reacting for 3 hours, the excess hydride is hydrolysed by dropwise addition of saturated aqueous NaCl solution. The reaction mixture is filtered, the solid is rinsed several times with THF and the filtrate is evaporated to yield a white meringue corresponding to the title compound.

Provenance & Evidence