HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 178526743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 4,6-Dichloro-5-nitropyrimidine | HCID 20312 | — |
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Product | HCID 178526743 | HCID 178526743 | — |
Reaction Steps
To a solution of 4,6-dichloro-5-nitro-pyrimidine (100 mg, 0.52 mmol) in anhydrous THF (2 mL) was added aminopyrazole (76 mg, 0.62 mmol). The solution was stirred at RT for 2 hrs and was filtered via short silica gel column. The filtrate that contained product and the unreacted starting pyrrimidine was concentrated under vacuum. The resulting residue was used directly without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07262200B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-eb0861f658c64e0dbed2f7cb1a384254 |
| Source note | uspto-grants-2007_08 |