HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69143566, compound → HCID 69144825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69143566 | HCID 69143566 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 69144825 | HCID 69144825 | 116% |
Reaction Steps
74 mg of tert-butyl [2-(2-hydroxymethylbenzofuran-5-ylamino)ethyl]methylcarbamate are dissolved in 10 ml of HCl/dioxane (4N) and stirred at room temperature for two hours. Evaporation in a rotary evaporator gives 59 mg of the desired product (HCl salt).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07262216B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-8a84de4f8f824d36a914999531ad47c5 |
| Source note | uspto-grants-2007_08 |