HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22938783, compound → HCID 22938670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22938783 | HCID 22938783 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22938670 | HCID 22938670 | 99.9% |
Reaction Steps
(2-ethoxy-4-nitrophenyl)(4-methylpyridin-2-yl)methanol (1.9 g) was dissolved in ethanol (100 ml), and the solution was reduced by catalytic hydrogenation with 10% palladium-carbon (0.2 g) of 50% hydration overnight. The catalyst was removed, and the solvent of the filtrate was evaporated to give (4-amino-2-ethoxyphenyl)(4-methylpyridin-2-yl)methanol (1.7 g) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07262185B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-9232da4786924d8eaef1edaf2fc01367 |
| Source note | uspto-grants-2007_08 |