HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69523111, compound → HCID 69521295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69523111 | HCID 69523111 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69521295 | HCID 69521295 | 95.7% |
Reaction Steps
4-[3-(4-nitrophenyl)propyl]-4H-1,2,4-triazole (1.2 g) was dissolved in ethanol (100 ml), 10% palladium-activated carbon (50% hydration, 0.2 g) was added to the solution at room temperature, and the solution was reduced by catalytic hydrogenation overnight. The catalyst was removed. The solvent of the filtrate was distilled off, to give 4-[3-(4-aminophenyl)propyl]-4H-1,2,4-triazole (1.0 g) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07262185B2 |
| Source dataset | uspto-grants-2007_08 |
| ORD ID | ord-6b73b53f496a496783a45c5d70e3f765 |
| Source note | uspto-grants-2007_08 |