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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 856810Generated: October 31, 2026

P-Anisidine → HCID 21862856, compound

https://huagongshe.com/reaction/856810

Reaction equation

Participants

RoleNameHCIDCharge
ReactantP-AnisidineHCID 7732—
Reactant4-(Methylsulfonyl)benzaldehydeHCID 220376—
SolventEthanolHCID 702—
ProductHCID 21862856HCID 2186285695%

Reaction Steps

1.00 g (5.4 mmol) of 4-methylsulfonylbenzaldehyde and 0.67 g (5.4 mmol) of 4-methoxyaniline were dissolved in 15 ml of ethanol, and the solution was heated under reflux for 1 hour. At the end of this time, the reaction solution was cooled to room temperature, and the crystals which precipitated were collected by filtration and washed with ethanol, to give 1.48 g (yield 95%) of the title compound as slightly yellow prismatic crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUSRE039420E1
Source datasetuspto-grants-2006_12
ORD IDord-d0fa0c38e45549d0b64364340fd7667e
Source noteuspto-grants-2006_12