HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrolein → N-(4-Methoxybenzylidene)-4-methylthioaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrolein | HCID 7847 | — |
| Reactant | alpha-(4-Methoxyphenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862854 | — |
| Product | N-(4-Methoxybenzylidene)-4-methylthioaniline | HCID 21862760 | — |
Reaction Steps
Following a procedure similar to that described in Example 21 (iii), but using α-(4-methoxyphenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as a white powder (yield 9%), melting at 183-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE039420E1 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-5be77a34cfbb4d90af8a382763010306 |
| Source note | uspto-grants-2006_12 |