HuagongsheHuagongshe Chemistry Print Report · For research reference only
Crotonaldehyde → alpha-(4-Difluoromethoxyphenyl)-alpha-(4-methylthioanilino)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Crotonaldehyde | HCID 447466 | — |
| Reactant | alpha-(4-Difluoromethoxyphenyl)-alpha-(4-methylsulfonylanilino)acetonitrile | HCID 21862740 | — |
| Product | alpha-(4-Difluoromethoxyphenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862794 | — |
Reaction Steps
Following a procedure similar to that described in Example 1(iii), but using α-(4-difluoromethoxyphenyl)-α-(4-methylsulfonylanilino)acetonitrile [prepared as described in step (ii) above] and crotonaldehyde as starting materials, the title compound was obtained as a white powder (yield 31%), melting at 98-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE039420E1 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-2aebb45d1c4140a6b49f0659aa90cf3d |
| Source note | uspto-grants-2006_12 |