HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroethane → HCID 91202882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroethane | HCID 6337 | — |
| Reactant | 1-Chloromethylnaphthalene | HCID 6845 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Product | HCID 91202882 | HCID 91202882 | 75% |
Reaction Steps
A mixture of 8.31 g (50 mmol) triethyl phosphite and 8.83 g (50 mmol) 1-chloromethyl naphthalene was heated for about 30 minutes until the evolution of gas (C2H5Cl) at 200° C. (external temperature) was finished. The reaction mixture was cooled to room temperature, to give 10.38 g NMPA (crude yield, 75%) as colorless oily liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144614B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-a13397a714f54be9a663159270a41482 |
| Source note | uspto-grants-2006_12 |