HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18440340, compound → HCID 66879498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18440340 | HCID 18440340 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 66879498 | HCID 66879498 | — |
Reaction Steps
(4S)-3(tert-Butyloxycarbonyl)thiazolidine-4-carboxamide (8.6 g, 37.1 mmol) was dissolved in 4M HCl/dioxan (50 ml). The mixture was stirred for 1 hour at room temperature then the solvent was evaporated in vacuo to give a white solid identified as (4R)-thiazolidinecarboxamide hydrochloride (6.2 g, 36.8 mmol, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144886B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-31191c59221f4d12925214dfe4658a33 |
| Source note | uspto-grants-2006_12 |