HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Benzyloxy)-N-methoxy-N-methylbenzamide → 3-hydroxy-N-methoxy-N-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Benzyloxy)-N-methoxy-N-methylbenzamide | HCID 21865361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-hydroxy-N-methoxy-N-methylbenzamide | HCID 21865376 | 98.4% |
Reaction Steps
To a solution of 100 g (0.37 mol) B1 in 750 ml tetrahydrofuran 10 g Pd/C (10%) were added and the mixture was hydrogenated at atmospheric pressure for 2 hours. The catalyst was filtered off and the filtrate was evaporated to yield 66.0 g B2 (98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144889B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-cf04c6ad9aa1470ca7ac83c55bd2b3a0 |
| Source note | uspto-grants-2006_12 |