HRID856967
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 100 g (0.37 mol) B1 in 750 ml tetrahydrofuran 10 g Pd/C (10%) were added and the mixture was hydrogenated at atmospheric pressure for 2 hours. The catalyst was filtered off and the filtrate was evaporated to yield 66.0 g B2 (98%).
WORKUP
后处理
- filtrationThe catalyst was filtered off
- customthe filtrate was evaporated