Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxylamine → HCID 178510916, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxylamine | HCID 787 | — |
| 반응물 | 3-(4-Chlorophenyl)prop-2-enenitrile | HCID 34243 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178510916 | HCID 178510916 | 51% |
반응 단계
A solution of 3-(4-chloro-phenyl)-acrylonitrile (1.63 g, 10 mmol) and hydroxyamine (0.74 ml, 12 mmol) in ethanol (10 ml) was stirred at room temperature overnight. The solvent was evaporated, and the residue was purified by column chromatography (EtOAc: Hexane=1:3) to give 1.0 g (51%) of 3-(4-chloro-phenyl)-N-hydroxy-acrylamidine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07144876B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-578bb4b3afc24da18386fd60f07449a6 |
| 출처 메모 | uspto-grants-2006_12 |