HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 482715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 1239093 | HCID 1239093 | — |
| Product | HCID 482715 | HCID 482715 | 67% |
Reaction Steps
To the sulfonamide (0.1 g) dissolved in methanol (2 mL) was added BTIB (1.1 eq.) in one portion as a solid. The resulting suspension was stirred at room temperature for 5 hours. The precipitate formed was collected on a filter, washed with ice cold methanol (2 mL) and dried under vacuum to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144893B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-b9532c42da3a4e60a77d47a657366abd |
| Source note | uspto-grants-2006_12 |