Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 857075Generated: October 28, 2026

Methanol → HCID 482715, compound

https://huagongshe.com/reaction/857075

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 1239093HCID 1239093—
ProductHCID 482715HCID 48271567%

Reaction Steps

To the sulfonamide (0.1 g) dissolved in methanol (2 mL) was added BTIB (1.1 eq.) in one portion as a solid. The resulting suspension was stirred at room temperature for 5 hours. The precipitate formed was collected on a filter, washed with ice cold methanol (2 mL) and dried under vacuum to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07144893B2
Source datasetuspto-grants-2006_12
ORD IDord-b9532c42da3a4e60a77d47a657366abd
Source noteuspto-grants-2006_12