HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21867058, compound → 6-[4-(3-Aminophenyl)butoxy]hexyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21867058 | HCID 21867058 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-[4-(3-Aminophenyl)butoxy]hexyl acetate | HCID 21867219 | 103.7% |
Reaction Steps
6-{[4-(3-Nitrophenyl)but-3-ynyl]oxy}hexyl acetate (2.973 g) was hydrogenated over PtO2 (300 mg) in EtOH over 1 h. The catalyst was removed by filtration and washed with EtOH. The combined filtrate and washings were concentrated under reduced pressure to give the title compound (2.844 g) LCMS RT=3.30 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144908B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-86418d09047148dd989cadad2369ca55 |
| Source note | uspto-grants-2006_12 |