HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 21865599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Isopropyl isocyanate | HCID 61277 | — |
| Reactant | HCID 10312400 | HCID 10312400 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21865599 | HCID 21865599 | — |
Reaction Steps
Prepared according to the procedure described in EXAMPLE 41 but using (1-{3-[6-(1-Methanesulfonyl-1-methyl-ethyl)-quinolin-8-yl]-phenyl}-ethyl)-(4-methylsulfanyl-phenyl)-amine (EXAMPLE 44, step 1) and iso-propyl isocyanate as the starting materials. Flash chromatography (CH2Cl2:EtOAc; 4:1) afforded the title compound as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144896B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-4188a09a9d56410b9c7be31c43be7742 |
| Source note | uspto-grants-2006_12 |