HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 10196916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 21865639 | HCID 21865639 | — |
| Product | HCID 10196916 | HCID 10196916 | — |
Reaction Steps
Prepared in two steps according to the procedures described in EXAMPLE 41 but using the {2-fluoro-5-[6-(1-methanesulfonyl-1-methyl-ethyl)-quinolin-8-yl]-benzyl}-(4-methanesulfonyl-phenyl)-amine from present Step 4 as the starting material. Flash chromatography (CH2Cl2:MeOH; 96:4) afforded the compound as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144896B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-160780dc175146949da53aa5c5453595 |
| Source note | uspto-grants-2006_12 |