HCID 69019756, compound → HCID 21865632, compound

HRID 857302Notes

Reaction equation

HRID 857302 reaction equation
C(OC(=O)[C:6]1[CH:11]=[CH:10][C:9]([O:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([C:20]3[CH:21]=[C:22]([CH:30]([CH3:32])[CH3:31])[CH:23]=[C:24]4[C:29]=3[N:28]=[CH:27][CH:26]=[CH:25]4)[CH:15]=2)=[CH:8][CH:7]=1)(C)C>CCOC(C)=O>[CH:30]([C:22]1[CH:23]=[C:24]2[C:29](=[C:20]([C:16]3[CH:15]=[C:14]([CH:19]=[CH:18][CH:17]=3)[CH2:13][O:12][C:9]3[CH:10]=[CH:11][C:6]([C:9]([OH:12])([CH3:10])[CH3:8])=[CH:7][CH:8]=3)[CH:21]=1)[N:28]=[CH:27][CH:26]=[CH:25]2)([CH3:32])[CH3:31]

Participants

3

Reactant 1

HCID 69019756HCID 69019756, compound

Product 1

HCID 21865632HCID 21865632, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Prepared according to the procedure described in EXAMPLE 11 but using the previous ester from step 1 as the starting material. Flash chromatography (Hex:EtOAc 0 to 70% gradient) afforded the compound as a foam.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-0a65f394f7d742c2b175c9f80e626482
Source dataset
uspto-grants-2006_12
Patent number
US07144896B2

Reaction notes

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