HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl[8-isopropenyl-6-(methylsulfonyl)-2,3-dihydro-1h-pyrrolo[1,2-a]indol-1-yl]acetate → Methyl[8-isopropyl-6-(methylsulfonyl)-2,3-dihydro-1H-pyrrolo[1,2-a]indol-1-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl[8-isopropenyl-6-(methylsulfonyl)-2,3-dihydro-1h-pyrrolo[1,2-a]indol-1-yl]acetate | HCID 90964995 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl[8-isopropyl-6-(methylsulfonyl)-2,3-dihydro-1H-pyrrolo[1,2-a]indol-1-yl)acetate | HCID 131726145 | — |
Reaction Steps
To the product of Step 2 (130 mg, 0.39 mmol) in EtOH (3 mL) was added Pd/C 10% (40 mg). The mixture was hydrogenated with a Parr hydrogenator at 50 psi for 45 minutes, filtered on a pad of celite, and the filtrate evaporated to dryness and used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144913B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-ae0198c4502b4bbb96c0fcbcff00c93e |
| Source note | uspto-grants-2006_12 |