HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 91379151, compound → HCID 91430685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 91379151 | HCID 91379151 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 91430685 | HCID 91430685 | — |
Reaction Steps
To the compound of Step 1 (200 mg, 0.67 mmol) in EtOH (20 mL) was added Pd/C 10% (100 mg). The mixture was hydrogenated with a Parr hydrogenator at 50 psi for 45 minutes the filtered on a pad of celite. The filtrate was evaporated to dryness and used as such in the next step (170 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144913B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-d7682efbd2dd4ee5bcddf5220621f35b |
| Source note | uspto-grants-2006_12 |