HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 12054423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4-(Trifluoromethyl)thiophenol | HCID 136653 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12054423 | HCID 12054423 | — |
Reaction Steps
To a solution of 4-(trifluoromethyl)benzenethiol (1 g) in Et2O was added bromine until orange color remained. The addition was stopped and the organic layer was washed with 1:1 aqueous saturated NaHCO3/10% aqueous Na2S203, dried over Na2SO4 and concentrated to give the title compound used as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144913B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-2f295d233665407dbf094ffbea2d6caa |
| Source note | uspto-grants-2006_12 |