HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90986359, compound → HCID 90963122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90986359 | HCID 90986359 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 90963122 | HCID 90963122 | 95.8% |
Reaction Steps
A mixture of the compound of Step 3 (78 mg) and 20 mg of Pd/C (10% w/w) in EtOH (3 mL) was stirred under H2 (balloon) for 1 h. The mixture was then filtered through a silica gel pad eluted with EtOAc and the filtrate was concentrated to give 75 mg of the title compound used as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07144913B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-67045c1e5660439bb9df273b8734a99d |
| Source note | uspto-grants-2006_12 |