Hydrochloric Acid → HCID 10119804, compound

Participants

Reaction Steps

The compound of Step 1 was dissolved in MeOH (2 mL) and 1,4-dioxane (2 mL) and treated with 1N LiOH for 2 h at room temperature. Addition of 1N NaH2PO4 (3 mL) and 1N HCl (0.4 mL) led to a suspension that was filtered through paper. The solid was air dried overnight yielding 14 mg of the title compound as a white solid.

Provenance & Evidence