化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | HCID 178453037 | HCID 178453037 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt | HCID 178479178 | — |
反応手順
Hydrogen chloride gas was bubbled through a 0° C. solution of tert-butyl 2-(1H-pyrazol-3-yl)benzylcarbamate (60 mg, 0.220 mmol) in ethyl acetate (5 ml) for 2 min and stirred for 40 min. A precipitate formed, and the suspension was concentrated in vacuo to give 2-(1H-pyrazol-3-yl)-benzylamine hydrochloride salt; MS (ES+) M+1 174.1 for C10H11N3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07144899B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-22a5083e6e1a44fdb08b7e75ca87b653 |
| 出典メモ | uspto-grants-2006_12 |