2,5-Dimethoxyaniline → HCID 135528620, compound

HRID 858211Notes

Reaction equation

HRID 858211 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[CH:8][C:7]([O:10]C)=[CH:6][C:4]=1[NH2:5].[F:12][C:13]1[CH:14]=[C:15]([CH:19]=[CH:20][C:21]=1[O:22]C)C(O)=O>>[F:12][C:13]1[CH:14]=[C:15]([C:1]2[O:2][C:3]3[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][C:4]=3[N:5]=2)[CH:19]=[CH:20][C:21]=1[OH:22]

Participants

3

Reactant 2

HCID 76132,5-DimethoxyanilineHCID 27334013-Fluoro-4-methoxybenzoic acid

Product 1

HCID 135528620HCID 135528620, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,5-dimethoxyaniline, and 3-fluoro-4-methoxybenzoic acid and was obtained as a white solid, m.p. 262–268° C.; MS m/e 244 (M−H)+.

Workup

  1. customwas obtained as a white solid, m.p. 262–268° C.

Sources & evidence

ORD record
ord-6b5e98e3325d43f9a5da4f626bb48d8a
Source dataset
uspto-grants-2006_12
Patent number
US07148247B2

Reaction notes

Loading…