HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxyaniline → 2-(3-Chloro-4-hydroxy-phenyl)-benzooxazol-5-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxyaniline | HCID 7613 | — |
| Reactant | 3-Chloro-p-anisic acid | HCID 169982 | — |
| Product | 2-(3-Chloro-4-hydroxy-phenyl)-benzooxazol-5-ol | HCID 135443280 | — |
Reaction Steps
The title compound was prepared in substantially the same manner as described in Example 1, from 2,5-dimethoxyaniline, and 3-chloro-4-methoxybenzoic acid and was obtained as a white solid, m.p. 254–256° C.; MS m/e 260 (M−H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148247B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-31a69f4bd9fa4290b39a2478112a5327 |
| Source note | uspto-grants-2006_12 |