2,3-Dimethoxybenzoic acid → HCID 135430305, compound

HRID 858217Notes

Reaction equation

HRID 858217 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[C:8]([O:10]C)[CH:7]=[CH:6][C:4]=1[NH2:5].C[O:13][C:14]1[C:22]([O:23]C)=[CH:21][CH:20]=[CH:19][C:15]=1C(O)=O>>[OH:10][C:8]1[CH:7]=[CH:6][C:4]2[N:5]=[C:1]([C:21]3[CH:20]=[CH:19][CH:15]=[C:14]([OH:13])[C:22]=3[OH:23])[O:2][C:3]=2[CH:9]=1

Participants

3

Reactant 2

HCID 152042,3-Dimethoxybenzoic acidHCID 176522,4-Dimethoxyaniline

Product 1

HCID 135430305HCID 135430305, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,4-dimethoxyaniline, and 2,3-dimethoxybenzoic acid and was obtained as a tan solid, m.p. 256–258° C.; MS m/e 244 (M+H)+.

Workup

  1. customwas obtained as a tan solid, m.p. 256–258° C.

Sources & evidence

ORD record
ord-347dcc92440f48898aecd0cb4ac8d9f7
Source dataset
uspto-grants-2006_12
Patent number
US07148247B2

Reaction notes

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