2,4-Dimethoxybenzoic acid → HCID 135486039, compound

HRID 858221Notes

Reaction equation

HRID 858221 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[CH:8][C:7]([O:10]C)=[CH:6][C:4]=1[NH2:5].C[O:13][C:14]1[CH:22]=[C:21]([O:23]C)[CH:20]=[CH:19][C:15]=1C(O)=O>>[OH:10][C:7]1[CH:8]=[CH:9][C:3]2[O:2][C:1]([C:20]3[CH:19]=[CH:15][C:14]([OH:13])=[CH:22][C:21]=3[OH:23])=[N:5][C:4]=2[CH:6]=1

Participants

3

Reactant 2

HCID 70522,4-Dimethoxybenzoic acidHCID 76132,5-Dimethoxyaniline

Product 1

HCID 135486039HCID 135486039, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,5-dimethoxyaniline, and 2,4-dimethoxybenzoic acid and was obtained as a white solid, m.p. greater than 300° C.; MS m/e 242 (M−H)+.

Workup

  1. customwas obtained as a white solid, m.p. greater than 300° C.

Sources & evidence

ORD record
ord-a655e8fc569447459040144c9dafa514
Source dataset
uspto-grants-2006_12
Patent number
US07148247B2

Reaction notes

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