p-Anisoyl chloride → HCID 135471161, compound

HRID 858222Notes

Reaction equation

HRID 858222 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[C:8]([O:10]C)[CH:7]=[CH:6][C:4]=1[NH2:5].C[O:13][C:14]1[CH:22]=[CH:21][C:17](C(Cl)=O)=[CH:16][CH:15]=1>>[OH:13][C:14]1[CH:22]=[CH:21][C:17]([C:1]2[O:2][C:3]3[CH:9]=[C:8]([OH:10])[CH:7]=[CH:6][C:4]=3[N:5]=2)=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 176522,4-Dimethoxyaniline

Product 1

HCID 135471161HCID 135471161, compound

Procedure

The title compound was prepared in substantially the same manner as described in Example 1, from 2,4-dimethoxyaniline, and 4-methoxybenzoyl chloride and was obtained as a white solid, m.p. greater than 300° C.; MS m/e 226 (M−H)+.

Workup

  1. customwas obtained as a white solid, m.p. greater than 300° C.

Sources & evidence

ORD record
ord-6b159b82be444defb857e47c6e6dec9c
Source dataset
uspto-grants-2006_12
Patent number
US07148247B2

Reaction notes

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