HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromothiophenol → 1-Bromo-4-(3-methylbut-2-enylsulphanyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromothiophenol | HCID 66049 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Product | 1-Bromo-4-(3-methylbut-2-enylsulphanyl)benzene | HCID 15096745 | 93% |
Reaction Steps
In a manner similar to that of Example 34(h), by reaction of 30.00 g (159.0 mmol) of 4-bromo-thiophenol with 26.00 g (175.0 mmol) of 1-bromo-3-methyl-2-butene, 37.40 g (93%) of the expected product are obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07148245B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-821253acb6c6473c9f050dc807a5a118 |
| Source note | uspto-grants-2006_12 |