反应详情

To a solution of ethyl(6-nitro-3-pyridinyl)acetate (468 mg, 2.60 mmol) in tetrahydrofuran was added LiAlH4 and stirred for 2 h at room temperature. The reaction was quenched with saturated 25% NH3 aqueous solution and the precipitate was removed. The filtrate was concentrated to give a title compound as yellow oil.

1. customThe reaction was quenched with saturated 25% NH3 aqueous solution
2. customthe precipitate was removed
3. concentrationThe filtrate was concentrated