Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 859147Generated: October 30, 2026

Sodium Hydroxide → HCID 69588346, compound

https://huagongshe.com/reaction/859147

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 69588313HCID 69588313—
SolventSulfuric AcidHCID 1118—
ProductHCID 69588346HCID 69588346—

Reaction Conditions

Temperature150 °C

Reaction Steps

Ethyl 7-(2,4-dichlorophenyl)-2,6-dimethylpyrazolo[1,5-a]pyridine-3-carboxylate (930 mg, 2.56 mmol) was treated with 50% H2SO4 (10 mL) and heated to 150° C. for 2.5 hours. The reaction was cooled in an ice bath and treated with 4N NaOH (19 mL) and NaHCO3 (4.80 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07151109B2
Source datasetuspto-grants-2006_12
ORD IDord-d3b5936ccae748d182f760113b31d778
Source noteuspto-grants-2006_12