HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 58763949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 58763940 | HCID 58763940 | — |
| Product | HCID 58763949 | HCID 58763949 | — |
Reaction Steps
A solution of 4-(2-tert-butoxycarbonylaminoethylamino)-1-(2-chlorophenyl)-5-(4-chlorophenyl)-1H-pyrazole-3-carboxylic acid (I-4c, 879 mg) in 2:1 conc HCl/EtOH (12 ml) was allowed to stand at room temperature for 17 hours. The reaction mixture was concentrated under vacuum to give the desired product I-4d: +ES MS (M+1) 391.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07151097B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-1334e5a173024bda8cccfca22638ab2d |
| Source note | uspto-grants-2006_12 |