Benzene, 1,2-dichloro-4-iodo- → HCID 69592819, compound

HRID 859276Notes

Reaction equation

HRID 859276 reaction equation
[C:1]([O:5][C:6](=[O:18])[NH:7][C:8]1[CH:13]=[CH:12][C:11](I)=[CH:10][C:9]=1[N+:15]([O-:17])=[O:16])([CH3:4])([CH3:3])[CH3:2].B1(B2OC(C)(C)C(C)(C)O2)OC(C)(C)C(C)(C)O1.[Cl:37][C:38]1[CH:39]=[C:40](I)[CH:41]=[CH:42][C:43]=1[Cl:44]>>[C:1]([O:5][C:6](=[O:18])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:41]2[CH:40]=[CH:39][C:38]([Cl:37])=[C:43]([Cl:44])[CH:42]=2)=[CH:10][C:9]=1[N+:15]([O-:17])=[O:16])([CH3:4])([CH3:3])[CH3:2]

Participants

4

Reactant 3

HCID 88591Benzene, 1,2-dichloro-4-iodo-HCID 2733548Bis(pinacolato)diboraneHCID 23554339Tert-butyl (4-iodo-2-nitrophenyl)carbamate

Product 1

HCID 69592819HCID 69592819, compound

Procedure

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 3,4-dichloro-iodobenzene according to the general procedure C. Obtained as a yellow solid (540 mg).

Sources & evidence

ORD record
ord-34a9dd6afa424481a118ac8d453eb6aa
Source dataset
uspto-grants-2006_12
Patent number
US07151098B2

Reaction notes

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