HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobiphenyl → (3''-Nitro-[1,1';4',1'']terphenyl-4''-yl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobiphenyl | HCID 7101 | — |
| Reactant | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | (3''-Nitro-[1,1';4',1'']terphenyl-4''-yl)-carbamic acid tert.-butyl ester | HCID 69592829 | — |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 4-bromobiphenyl according to the general procedure C. Obtained as a yellow solid (1.29 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07151098B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-e5169c6bdced4148b56bed1bcf225590 |
| Source note | uspto-grants-2006_12 |