HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → HCID 69592764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | HCID 69592839 | HCID 69592839 | — |
| Product | HCID 69592764 | HCID 69592764 | 97% |
Reaction Steps
Prepared from (2-nitro-4-p-tolylethynyl-phenyl)-carbamic acid tert.-butyl ester (Example F4) (640 mg, 1.82 mmol) by reduction with SnCl2.2H2O (2.0 g, 9.1 mmol) according to the general procedure G (method b). Obtained as a beige solid (569 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07151098B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-c8f079c8b94d492889e73881ec56748b |
| Source note | uspto-grants-2006_12 |