Stannous chloride dihydrate → HCID 69592808, compound

HRID 859336Notes

Reaction equation

HRID 859336 reaction equation
[C:1]([O:5][C:6](=[O:25])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][C:17]([C:20]#[N:21])=[CH:16][CH:15]=2)=[CH:10][C:9]=1[N+:22]([O-])=O)([CH3:4])([CH3:3])[CH3:2].O.O.Cl[Sn]Cl>>[C:1]([O:5][C:6](=[O:25])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][C:17]([C:20]#[N:21])=[CH:16][CH:15]=2)=[CH:10][C:9]=1[NH2:22])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 61436Stannous chloride dihydrateHCID 69592863(4'-Cyano-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester

Product 1

HCID 69592808HCID 69592808, compound

Procedure

Prepared from (4′-cyano-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example C13) by reduction with SnCl2.2H2O according to the general procedure G (method b). Obtained as a yellow solid (360 mg).

Sources & evidence

ORD record
ord-4c692c09abb44318b3e2deab1187b9a7
Source dataset
uspto-grants-2006_12
Patent number
US07151098B2

Reaction notes

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