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HRID859358

反应详情

EQUATION

反应方程式

HRID 859358 的结构方程式

REACTANTS

反应物

4
结构：O=C(O)c1cccc(-n2cnnn2)c1
HCID750220

3-(1H-tetrazol-1-yl)benzoic acid

C8H6N4O2

结构：CCOC(=O)CC(=O)[O-].[K+]
HCID3446434

Potassium ethyl malonate

C5H7KO4

结构：[Cl-].[Cl-].[Mg+2]
HCID5360315

Magnesium Chloride

Cl2Mg

结构：CCN(CC)CC.CCOC(=O)Cl
HCID19692316

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CC(=O)c1cccc(-n2cnnn2)c1
HCID69592791

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

Prepared from 3-tetrazol-1-yl-benzoic acid [CAS-No. 204196-80-5] by activation with ethyl chloroformate/Et3N and reaction with ethyl malonate potassium salt with Et3N and MgCl2 in CH3CN according to general procedure H (method a). Obtained as a light yellow solid (211 mg).