HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Amino-4-phenylethynyl-phenyl)-carbamic acid tert-butyl ester → HCID 86587994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Amino-4-phenylethynyl-phenyl)-carbamic acid tert-butyl ester | HCID 11404065 | — |
| Reactant | HCID 22224697 | HCID 22224697 | — |
| Product | HCID 86587994 | HCID 86587994 | 101% |
Reaction Steps
Prepared from (2-amino-4-phenylethynyl-phenyl)-carbamic acid tert.-butyl ester (Example G2) (1.0 g, 3.24 mmol) and 6-(3-iodo-phenyl)-2,2-dimethyl-[1,3]dioxin-4-one (Example J7) (1.78 g, 3.57 mmol) according to the general procedure K. Obtained as a light yellow solid (1.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07151098B2 |
| Source dataset | uspto-grants-2006_12 |
| ORD ID | ord-f7f19ddd0d0e42769addb7dc0bb02a42 |
| Source note | uspto-grants-2006_12 |